The structure of phenol - Arn „ n = 1 , 2 )
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Crystal Structure of Schiff base Compound 2-[(2-chloro-4-nitrophenyl) iminomethyl] phenol
Single crystals of Schiff base compound 2-[(2-chloro-4-nitrophenyl) iminomethyl] phenol (1) were grown by the slow evaporation technique at room temperature. The crystal structure of the title compound was determined by single crystal X-ray diffraction. The title compound crystallizes in the monoclinic system, space group P21, with two symmetry independent molecules. Intramolecular O-H···N hydr...
متن کاملChromium complexes bearing amidinato-phosphino ligand: synthesis, characterization, and catalytic properties of ethylene tri-/tetramerization and polymerization.
An amidinato-phosphino ligand ArN[double bond, length as m-dash]C(R)NH(o-Ph2PC6H4) (Ar = 2,4,6-Me3C6H2, R = Ph (1); Ar = 2,6-iPr2C6H3, R = Ph (2); Ar = 2,6-iPr2C6H3, R = tBu (3)) was prepared. The ligand reacted with CrCl3(THF)3 to yield the N,P-chelation complex [ArNHC(R)[double bond, length as m-dash]N(o-Ph2PC6H4)]CrCl3(THF) (4-6), and the ligand's lithium salt ArN[double bond, length as m-da...
متن کاملMicrosolvation of HN2 in Argon: Infrared Spectra and ab Initio Calculations of Arn-HN2 (n ) 1-13)
Infrared (IR) photodissociation spectra of mass selected Arn-HN2 complexes (n ) 1-13) have been recorded in the 4 μm spectral range in a tandem mass spectrometer. The dominant features are assigned to the ν1 + mνs (m ) 1, 2) combination bands, where ν1 corresponds to the intramolecular N-H stretch mode and νs to the intermolecular stretching vibration of the first (proton-bound) Ar ligand. Syst...
متن کاملCrystal structure of unsymmetrical α-diimine palladium(II) complex cis-[{ArN=C(Me)–(Et)C=NAr}PdCl2] [Ar = 2,6-(iPr)2C6H3]
The unsymmetrical α-di-imine ligand N-{2-[2,6-bis-(propan-2-yl)phenylimino]pentan-3-yl-idene}-2,6-bis-(propan-2-yl)aniline, [ArN=C(Me)-(Et)C=NAr] [Ar = 2,6-(iPr)2C6H3], (I), and the corresponding palladium complex, cis-(N-{2-[2,6-bis-(propan-2-yl)phenylimino]pentan-3-yl-idene}-2,6-bis-(propan-2-yl)aniline)di-chlor-ido-palladium(II) 1,2-di-chloro-ethane monosolvate, [PdCl2(C29H42N2)]·C2H4Cl2 or ...
متن کاملTime required for effective action of phenol against giant cell tumour cells.
PURPOSE To evaluate the time required for effective action of phenol against the giant cell tumour (GCT) cells. METHODS Fresh GCT cells were harvested from 9 patients with primary GCT of the distal femur (n=4), proximal tibia (n=4), and proximal humerus (n=1), with the Campanacci tumour grades 3 (n=6), 2 (n=2), and 1 (n=1). Specimens were immersed in 80 % phenol for one, 3, 6, and 10 minutes,...
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تاریخ انتشار 2017